Solvent extraction: effect of pH

Step 1
Contacting the fermentation broth with immiscible organic solvent such as MIBK.

The pH is adjusted just prior to mixing with the organic solvent. The product has a carboxyl group that makes it water soluble when ionized. When the -COOH is not ionized, the product prefers to be in an non-polar organic solvent. Assume that pK=5. Within roughly one pH unit, the concentration of product will depend on satisfying the distribution coefficient. Remember that when pH = pK, the compound is one-half ionized, but the solvent can get part of it as the equilibrium supplies more.
Enter the pH:
Broth: Solvent:

Step 2
Contacting solvent extract with aqueous solution.

Enter the pH:
Solvent: Water:

Review of ionic equilibria.

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created March 1997